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To a solution of 2. The lower phase had become quite solid and chunky. The combined decantation and ether washes were stripped of solvent on the rotary evaporator to yield a white solid residue with a brown oil contamination. The extracts were pooled and taken to dryness on the rotary evaporator to give 0. With scratching and stirring, crystals began to form slowly. This was removed by filtration, washed with ether, and air dried to constant weight. There was thus obtained 0. The infra-red spectrum of the free base contained the following major peaks cm For the hydrochloride salt cm


Post Introduction Cluster headaches are a primary headache disorder characterized by intense unilateral head pain, localized in the supraorbital or suborbital regions. The pain of cluster headaches is frequently debilitating, and some patients have been driven to suicide as a means to escape their suffering. Front-line medications to treat cluster headaches are limited. At present, there are no pharmaceuticals developed specifically to treat cluster headache symptoms.

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To a solution of 1. The solution which became cloudy in 20 minutes was stirred at ambient temperature for 12 hrs. The dark red solids that formed were broken up mechanically and, after they had settled, the overhead liquid was removed by decantation. The remaining solids were washed with 30 mL anhydrous ether, and these washings were combined with the decanting and the volatiles were removed on the rotary evaporator. The crude isolate was dissolved in 1.

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The short version is that 5-MeO-DALT is a fairly new option for cluster headache patients who are comfortable self-administering treatments. It is a simple tryptamine that acts on serotonin receptors in the brain. When used carefully, 5-MeO-DALT is extremely safe and is proving to be very effective for some cluster headache patients. Who invented this cluster headache treatment? Nobody invented it as a cluster headache treatment at all.

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